I-Palladium CAS: 7440-05-3 iPowder emnyama
| Inombolo Yekhathalogu | XD90595 |
| Igama lemveliso | I-Palladium |
| CAS | 7440-05-3 |
| Ifomula yeemolekyuli | Pd |
| Ubunzima beMolekyuli | 106.42 |
| Iinkcukacha zokuGcina | I-Ambient |
| IKhowudi yoMrhumo eHarmonized | 38151200 |
Ukucaciswa kweMveliso
| Imbonakalo | Umgubo omnyama |
| Isivavanyi | 99% |
| Amanzi | 70% max |
| IR | <0.001% |
| AS | 0.002% |
| Fe | <0.001% |
| Cu | <0.001% |
| Pb | <0.001% |
| Cd | <0.001% |
| Zn | 0.001% |
| Ni | 0.001% |
| Mg | <0.001% |
| Al | <0.001% |
| Si | <0.001% |
| Cr | <0.001% |
| Co | <0.001% |
| Pd | 4.95% |
| Sb | 0.001% |
| Mn | <0.001% |
| Pt | <0.001% |
| Rh | <0.001% |
| Au | <0.001% |
| Ag | <0.001% |
| Sn | 0.001% |
| Mo | <0.001% |
| Bi | <0.001% |
| Ti | <0.001% |
| W | 0.001% |
| Zr | <0.001% |
| V | <0.001% |
| Ru | <0.001% |
| Indawo ethile yomphezulu | >970m2/g |
Umsebenzi okhoyo uxela inoveli inyathelo elinye, iprotocol eluhlaza yokwenziwa kwe-starch-stabilized palladium nanoparticles (PdNPs) kunye ne-particle diameter ye-30-40 nm.La masuntswana azinzile kwaye alinganayo ngobukhulu.Kwiprothokholi yangoku, ukuncitshiswa kwe-solar edibeneyo yokunciphisa i-palladium chloride kwaphunyezwa ngokusebenzisa i-citric acid njenge-agent yokunciphisa kunye ne-starch njenge-agent agent.I-UV-Visible spectroscopy, i-Transmission Electron Microscopy, i-Field Emission Gun-Scanning Electron Microscopy, Indawo ekhethiweyo ye-Electron Diffraction kunye ne-Electron dispersive X-ray ubuchule bokuhlalutya be-Spectral busetyenziselwe ukubonakalisa le PdNP ye-starch caped.Apha;sibika ukudibanisa okunjalo kwesitashi kunye ne-citric acid kwi-synthesis ye-PdNPs okokuqala.Umsebenzi we-catalytic we-nanoparticles eyenziwe yajongwa kwi-Suzuki kunye ne-Heck cross coupling reactions.Imveliso yemveliso yaqinisekiswa yiGC.Iimveliso zaqinisekiswa kusetyenziswa uhlalutyo lwe-GC-MS kunye nokusebenzisa i-GC kunye nemigangatho yokwenyani.Amandla elanga ancedise isitashi esizinzile iiPdNPs zibonise umsebenzi ogqwesileyo kwi-CC bond formation phakathi kwe-aryl halides (I, Br) kunye ne-phenyl boronic acid kunye ne-derivatives yayo.Ukongeza, i-catalyst ibonise umsebenzi omhle kwi-Heck coupling reaction ye-CC bond formation ye-aryl halides ene-alkene enuka kamnandi.Ukusetyenziswa kwesitatshi, i-citric acid, amanzi kunye namandla elanga kwenza inkqubo ekhoyo ngoku ibe luhlaza.
