4,4-bis(Dimethylamino)thiobenzophenone CAS:1226-46-6 Ubunzulu obuqinileyo obubomvu
| Inombolo Yekhathalogu | XD90453 |
| Igama lemveliso | 4,4-bis(Dimethylamino)thiobenzophenone |
| CAS | 1226-46-6 |
| Ifomula yeemolekyuli | I-C17H20N2OS2 |
| Ubunzima beMolekyuli | 284.42 |
| Iinkcukacha zokuGcina | 2 ukuya ku-8 °C |
| IKhowudi yoMrhumo eHarmonized | 29309099 |
Ukucaciswa kweMveliso
| Indawo yokunyibilika | 202 - 206 Deg C |
| Ubunyulu (HPLC) | 99% |
| Kubuntununtunu begolide | Iyahambelana |
| Uvavanyo lweChloroform yokunyibilikisa | Iyahambelana |
| Imbonakalo | Ubunzulu obubomvu buqinile |
Indlela elula, inoveli kunye ne-ebucayi ye-spectrophotometric yachazwa ngokumisela kwangaxeshanye i-mercury kunye ne-palladium.Indlela isekelwe ekubunjweni okunzima kwe-mercury kunye ne-palladium kunye ne-Thio-Michler's Ketone (TMK) kwi-pH 3.5.Zonke izinto ezichaphazela ubuntununtunu ziye zaphuculwa kwaye uluhlu oluguquguqukayo oluhambelana nokumisela i-mercury kunye ne-palladium ifunyenwe.Ukuzimisela kwangaxeshanye imixube ye-mercury kunye ne-palladium ngokusebenzisa indlela ye-spectrophotometric yingxaki enzima, ngenxa yokuphazamiseka kwe-spectral.Ngeendlela zokulinganisa i-multivariate ezifana nezikwere ezincinci (i-PLS), kunokwenzeka ukuba ufumane imodeli ehlengahlengisiweyo kumaxabiso okuxininisa imixube esetyenziswe kuluhlu lokulinganisa.Ukulungiswa komqondiso we-Orthogonal (OSC) bubuchule bokucubungula kwangaphambili obusetyenziselwa ukususa ulwazi olungahambelani noguquko ekujoliswe kulo olusekwe kuhlalutyo olunyanzelweyo lwecandelo eliyintloko.I-OSC yindlela efanelekileyo yokulungiswa kwangaphambili kwe-PLS yokulinganisa imixube ngaphandle kokulahlekelwa ngumthamo wokuqikelela usebenzisa indlela ye-spectrophotometric.Kule sifundo, imodeli yokulinganisa isekelwe kwi-spectra yokufunxa kwi-360-660 nm uluhlu lwe-25 imixube eyahlukeneyo ye-mercury kunye ne-palladium.Iimatriki zokulinganisa zaziqukethe i-0.025-1.60 kunye ne-0.05-0.50 microg mL (-1) ye-mercury kunye ne-palladium, ngokulandelanayo.I-RMSEP ye-mercury kunye ne-palladium ene-OSC kwaye ngaphandle kwe-OSC yayiyi-0.013, 0.006 kunye ne-0.048, 0.030, ngokulandelanayo.Le nkqubo ivumela ukuzimisela ngaxeshanye mercury kunye palladium kwi zokwenziwa kunye neesampulu real matrix ukuthembeka okulungileyo ukuzimisela.
